@article { author = {Shakir.Turkie, Nagham and Naeem Abd Oun, Zahraa}, title = {Development of a new methodology for Lincomycin.HCI (LINO.HCI) determination using phosphomolybdic acid (PMA) as a reagent and ISNAG-Fluorimeter Instrument via CFIA}, journal = {Asian Journal of Green Chemistry}, volume = {6}, number = {1}, pages = {88-102}, year = {2022}, publisher = {Sami Publishing Company}, issn = {2588-5839}, eissn = {2588-4328}, doi = {10.22034/ajgc.2022.1.7}, abstract = {The reaction is based on the Lincomycin that has been responded. In an acidic solution, combine HCl and phosphomolybdic acid to produce a white color precipitate that may be measured using an ISNAG-Fluorimeter (homemade instrument). Some chemical and physical variables have been evaluated. The correlation coefficient was r=0.9983. The calibration curve was linear (the range was 0.0051 mmol/L). The minimum detection limit concentration in the linear dynamic range of the calibration curve was 19.935 ng. The RSD percent of lincomycin HCl at 0.3 and 0.8 mmol/L was less than 0.25% (n=8). The approach was used to determine lincomycin HCl in three pharmaceutical tablets. Comparisons were made using a standard expansion approach and a matched t-test between the recently created method and the traditional strategy (UV-Vis spectrophotometry and turbidimetry with a turbidimeter). At the 95% confidence level, there was no significant difference between the two techniques.}, keywords = {Lincomycin HCl Flow injection Scatter light ISNAG,Fluorimeter instrument}, url = {https://www.ajgreenchem.com/article_147371.html}, eprint = {https://www.ajgreenchem.com/article_147371_ce4d3ef3caf2dd804c84e68b2640423f.pdf} }